By Clarence Karr
Analytical equipment for Coal and Coal items, quantity III, is the 3rd of a three-volume treatise that goals to supply an in depth presentation of what constitutes the 1st accomplished reference paintings dedicated completely to the topic of analytical technique for coal and coal items. the 3 volumes were divided right into a overall of twelve components, every one half containing a number of chapters dedicated to a specific topic. the current quantity offers with gases, waste items, by-products, environmental difficulties, and miscellaneous analytical difficulties, in addition to detailed instrumental thoughts for fixing quite a few difficulties.
Because varied points of a specific topic are often scattered via a number of chapters within the volumes, cross-references among chapters were entered. additionally, the topic indexes were made as particular as was once functional, and the reader will take advantage of exam of pertinent matters within the indexes of all 3 volumes. A cautious interpreting of those volumes will express that definitive recommendations aren't but to be had in a few cases. there's a transparent desire for persevered study at the basics of research of coal and coal items, and the improvement of trustworthy and actual analytical instrumentation, together with on-stream purposes.
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Additional info for Analytical Methods for Coal and Coal Products. Volume III
7. 39. 9898 C20 C2H30 C7H50 CHO2 C302 C=C=0+. Ion of C n H 2 n . 4 0 compounds Diagnostic of CH3CO—R compounds Diagnostic of aromatic CHO compounds Diagnostic of R—COOH compounds (acids) 0=C=C=C=0+. 9898 C20 C2H30 C2H50 C=C=0+. Ion of C nH2 n-*0 compounds Diagnostic of CH3CO—R compounds Diagnostic of H0CH2CH2—R compounds Diagnostic of C2H5—CO—R compounds Diagnostic of aromatic CHO compounds Diagnostic of R—COOH compounds (acids) 0=C=C=C=0+. 9898 C20 C2H30 C2H50 C2HO Oxygen 10mina a b C3H5O C7H5O CHO2 c3o2 C3H3O C3H50 C3H70 C4H70 C6H50 C7H50 CH0 2 C3O2 C=C—0+.
00116 The low-resolution mass spectrometer was operated under the conditions shown in Table II. The high-resolution mass spectrometer was operated as shown in Table III. III. A. DATA PROCESSING Interpretations of Bleuler Mill Data The volume of the gas-collecting system was determined to be 850 mliter. The samples were ground in duplicate and duplicate analyses of the collected gases were made by low-resolution mass spectrometry. The weight percent methane was obtained by using the ideal gas law and converting the gas to milliliters at standard conditions, then to liters, moles, grams, and finally to weight percent.
In the flame photometric Chromatograph (FPD), a 600 /xliter sample of coke oven gas is injected by the sample valve onto the g x 12 in. Teflon column, containing 100/ 120 mesh Teflon-6 coated with 5% SF-96, a methyl silicone stationary phase. The sulfur compounds pass through the column and backflush valve onto the second column, leaving behind oils, naphthalene, tar, and water. On a signal from the control system, the sample valve and 38. 25 Coke Oven Gas Analysis Flame Photometric Detector For COS, CS2 And SO, H2S To Vent Selector Valve £ 1/8- in.